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https://hdl.handle.net/10316/27498| Title: | 3-(Ammoniomethyl)pyridinium bis(perchlorate) | Authors: | Bayar, Imen Kefi, Riadh Silva, Pedro Sidónio Pereira da Silva, Manuela Ramos |
Keywords: | single-crystal X-ray study; T = 293 K; mean (C–C) = 0.003 A; R factor = 0.051; wR factor = 0.148; data-to-parameter ratio = 21.5 | Issue Date: | 2013 | Citation: | BAYAR, Imen [et. al] - 3-(Ammoniomethyl)pyridinium bis(perchlorate). "Acta Crystallographica Section E". ISSN 1600-5368. Vol. 69 (2013) | Serial title, monograph or event: | Acta Crystallographica Section E | Volume: | 69 | Abstract: | In the title molecular salt, C6H10N2 2+ 2ClO4 , the Cl—O bond lengths [anion 1: 1.369 (3)–1.415 (3); anion 2: 1.420 (2)– 1.441 (2) A ° ] and the O—Cl—O angles [anion 1: 105.4 (2)– 111.8 (4); anion 2: 107.8 (1)–110.3 (1) ] indicate a slight distortion of the perchlorate anions from regular tetrahedral symmetry. In the crystal, the components are linked into columns along the a-axis direction via N—H O and C— H O hydrogen bonds, with stacks of the organic molecules being surrounded by stacks of perchlorate anions. | URI: | https://hdl.handle.net/10316/27498 | ISSN: | 1600-5368 | DOI: | 10.1107/S1600536813012038 | Rights: | openAccess |
| Appears in Collections: | FCTUC Física - Artigos em Revistas Internacionais |
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| 3-(Ammoniomethyl)pyridinium.pdf | 542.21 kB | Adobe PDF | View/Open |
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