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https://hdl.handle.net/10316/4523| Title: | Crystal structure of hydrated diphenylguanidinium hexafluoroferrate (III) | Authors: | Silva, Manuela Ramos Beja, Ana Matos Costa, Benilde F. O. Paixão, José A. Veiga, Luiz Alte da |
Keywords: | Hydrated diphenylguanidinium hexafluoroferrate; Hydrated iron trifluoride; X-ray structure determination; X-ray powder diffraction; Mössbauer spectroscopy | Issue Date: | 2000 | Citation: | Journal of Fluorine Chemistry. 106:1 (2000) 77-81 | Abstract: | The crystal structure of 3C13H14N3+FeF63-·3.5H2O was determined. Both phenyl rings of the diphenylguanidine cation are oriented syn to the central C=NH2 group. The anions and cations are held together by a three-dimensional network of hydrogen bonds. In the synthesis of this compound, a second phase (iron trifluoride trihydrate) was formed and identified by powder diffraction data. Mössbauer results show two different iron environments compatible with the two phases reported. | URI: | https://hdl.handle.net/10316/4523 | DOI: | 10.1016/S0022-1139(00)00312-2 | Rights: | openAccess |
| Appears in Collections: | FCTUC Física - Artigos em Revistas Internacionais |
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| file9435186af2894cda906b5af598ef1fe0.pdf | 207.12 kB | Adobe PDF | View/Open |
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