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The authors acknowledge financial support from Fundação para a Ciência e Tecnologia (FCT) in the form of fellowships to PMA (SFRH/BD/69238/2010), IV (SFRH/BPD/90032/2012) and JAA (SFRH/BPD/91527/2012) and research Project CGL2017-89009-P. NMR data were collected at the UC-NMR facility that is supported by FEDER and FCT (RECI/QEQ-QFI/0168/2012, CENTRO-07-CT62-FEDER-002012) and Rede Nacional de Ressonância Magnética Nuclear (RNRMN). This study benefited from funding by the strategic program of MARE, financed by FCT (UID/MAR/04292/2019), and by FTC/MCTES to CESAM, (UID/AMB/50017 – POCI- 01-0145-FEDER-007638), through national funds.